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77% reduced molybdenum-red isopolyoxomolybdate was synthesized via solvothermal one-pot method and characterized by multiple spectroscopic techniques. The dataset includes results from single-crystal XRD, IR, Raman, UV-vis, TGA, and initial biocompatibility assays. Ingrid Gregorovic published the data on figshare in March 2026 under a CC-BY-4.0 license.
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