Analytical Method Validation for 23 Alkaloids in Flower Extract Supplements

A database supporting a study on a micro-solid phase extraction method for alkaloid detection. It includes UHPLC-MS parameters, validation results, matrix effect data, and AGREEprep scores for the methodology. The dataset, authored by Begoña Fernández-Pintor, was last updated on October 14, 2025.

Use Cases

• Validate analytical methodologies for alkaloid detection based on the included AGREEprep scores and validation results.
• Compare extraction efficiency between different techniques based on the table comparing this methodology to others in literature.
• Assess matrix effects in complex samples based on the reported recovery percentages and solvent-based calibration curves.
• Optimize micro-solid phase extraction procedures based on the results for the uSPEed(r) extraction optimization.

Strengths

• Includes a comprehensive validation suite covering matrix effects, recovery percentages, and AGREEprep scores.
• Provides a direct comparison of the proposed methodology against other techniques found in the scientific literature.
• Focuses on a specific application for 23 alkaloids in flower-based dietary supplements.

Limitations

• Column-level documentation is absent; field semantics must be inferred after download.
• Row count is unknown, which may limit suitability assessment for large-scale ML tasks.
• The dataset's primary focus is method validation, which may limit direct use for predictive modeling without additional context.

Provenance

Source

e-cienciaDatos Harvested Dataverse

Collection Method

Likely contains experimental results from laboratory analysis using UHPLC-MS and micro-solid phase extraction.

Time Range

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Freshness

Last updated 2025-10-14 21:43:34; freshness should be verified.

Geography

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